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| | Acetoxime O-(2,4,6-trimethylphenylsulfonate) Basic information |
| Product Name: | Acetoxime O-(2,4,6-trimethylphenylsulfonate) | | Synonyms: | Acetone O-(2,4,6-Trimethylphenylsulfonyl)oxime
O-(2,4,6-Trimethylphenylsulfonyl)acetoxime;tert-AMyl Ethyl Ether,1,1-DiMethylpropyl Ethyl Ether;Acetoxime O-(2,4,6-Trimethylphenylsulfonate);O-(2,4,6-TRIMETHYLPHENYLSULFONYL)ACETOXIME;Acetoxime O-(2,4,6-trimehylphenylsulfonate);Acetoximetrimehylphenylsulfonate;ACETONE O-(2,4,6-TRIMETHYLPHENYLSULFONYL)OXIME;Acetoxime O-(2,4,6-Trimethylphenylsulfonate) > | | CAS: | 81549-07-7 | | MF: | C12H17NO3S | | MW: | 255.33 | | EINECS: | | | Product Categories: | Amination;Synthetic Organic Chemistry | | Mol File: | 81549-07-7.mol |  |
| | Acetoxime O-(2,4,6-trimethylphenylsulfonate) Chemical Properties |
| Melting point | 96 °C | | Boiling point | 366.4±52.0 °C(Predicted) | | density | 1.13±0.1 g/cm3(Predicted) | | solubility | sol ether, THF; slightly sol benzene; insol hexane | | form | powder to crystal | | color | White to Almost white |
| | Acetoxime O-(2,4,6-trimethylphenylsulfonate) Usage And Synthesis |
| Preparation | Preparative Method: Acetone reacts with Hydroxylamine hydrochloride in methanol-aq. NaOH solution to yield acetoxime, which is also commercially available. Acetoxime reacts with 2,4,6- trimethylbenzenesulfonyl chloride in triethylamine-DMF to yield acetoxime O-(2,4,6- trimethylphenylsulfonyl)sulfonate. | | Uses | ACETOXIME O-(2,4,6-TRIMETHYLPHENYLSULFONATE) is an electrophilic aminating reagent for Grignard reagents. |
| | Acetoxime O-(2,4,6-trimethylphenylsulfonate) Preparation Products And Raw materials |
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