DICHLORO-N-DODECYLMETHYLSILANE(18407-07-3) MS

Product NameDICHLORO-N-DODECYLMETHYLSILANE

CAS 18407-07-3

Molecular FormulaC13H28Cl2Si

Molecular Weight283.35

InChIInChI=1S/C13H28Cl2Si/c1-3-4-5-6-7-8-9-10-11-12-13-16(2,14)15/h3-13H2,1-2H3

InChIKey ZAADUWCLWTWDSZ-UHFFFAOYSA-N

SmilesC(CC[Si](Cl)(Cl)C)CCCCCCCCC

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-7607          
dichlorododecylmethylsilane
C13H28Cl2Si         (Mass of molecular ion:    282)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       5.6
      28.0       1.2
      29.0      15.2
      36.0       2.0
      39.0       4.4
      41.0      31.2
      42.0       9.5
      43.0      74.0
      44.0       2.7
      53.0       1.8
      54.0       3.5
      55.0      22.7
      56.0      19.0
      57.0      91.1
      58.0       5.0
      63.0       3.3
      65.0       1.3
      67.0       2.7
      68.0       2.8
      69.0      19.2
      70.0      18.7
      71.0      64.4
      72.0       3.6
      78.0       1.7
      79.0       4.9
      81.0       1.9
      82.0       4.1
      83.0      12.8
      84.0      14.5
      85.0      44.9
      86.0       2.8
      93.0       1.7
      96.0       2.5
      97.0      11.1
      98.0      11.3
      99.0      12.8
     101.0       1.0
     105.0       1.8
     107.0       1.1
     110.0       1.3
     111.0       7.3
     112.0       6.8
     113.0     100.0
     114.0       7.3
     115.0      69.6
     116.0       4.5
     117.0      13.2
     119.0       3.4
     121.0       1.3
     125.0       3.6
     126.0       3.3
     127.0       2.6
     133.0       2.5
     135.0       1.0
     139.0       1.6
     140.0       4.7
     141.0      63.8
     142.0       5.6
     143.0      43.2
     144.0       3.6
     145.0       7.8
     147.0       9.5
     148.0       1.4
     149.0       3.4
     154.0       6.1
     155.0      31.0
     156.0       7.1
     157.0      20.9
     158.0       2.7
     159.0       4.0
     161.0       5.2
     163.0       1.9
     167.0       1.7
     168.0      12.0
     169.0      18.4
     170.0       2.7
     171.0      12.0
     172.0       1.3
     173.0       2.2
     182.0       1.1
     183.0       9.0
     184.0       1.7
     185.0       5.9
     187.0       1.1
     197.0       5.5
     198.0       1.0
     199.0       3.7
     211.0       3.1
     213.0       2.2
     225.0       3.0
     227.0       2.0
     239.0       2.6
     241.0       1.8
     246.0       2.6
     247.0       1.4
     248.0       1.1
     253.0       2.2
     255.0       1.6
     267.0       8.1
     268.0       1.6
     269.0       5.7
     270.0       1.0
     271.0       1.1
     282.0      10.5
     283.0       2.1
     284.0       7.3
     285.0       1.4
     286.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₂₈ Cl₂ Si	0.05 ml : 0.5 ml CDCl₃
dichlorododecylmethylsilane

    Assign.     Shift(ppm)

      A             1.492
      B             1.37
      C             1.27
      D             1.108
      E             0.880
      F             0.757

     Hz     ppm     Int.

    607.79   1.521     36
    600.10   1.502     60
    599.00   1.499     53
    596.19   1.492     32
    594.48   1.488     41
    592.16   1.482     66
    589.23   1.475     36
    584.47   1.463     30
    554.69   1.388     41
    547.61   1.371     55
    540.77   1.354     47
    540.41   1.353     47
    533.45   1.335     42
    520.75   1.304    104
    505.49   1.265   1000
    450.44   1.128    142
    445.07   1.114     56
    441.89   1.106     81
    434.08   1.087    115
    359.01   0.899    116
    352.29   0.882    360
    345.34   0.865    147
    302.61   0.758    966

in CDCl3