3-AMINO-2-METHOXYDIBENZOFURAN(5834-17-3) IR2

Product Name3-AMINO-2-METHOXYDIBENZOFURAN

CAS 5834-17-3

Molecular FormulaC13H11NO2

Molecular Weight213.23

Request For Quotation

Mass

MS-IW-0025          
2-methoxy-3-dibenzofuranamine
C13H11NO2           (Mass of molecular ion:    213)

   Source Temperature: 180 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      70.5       1.8
      77.0       1.0
      85.0       4.5
     106.5       4.5
     114.0       1.3
     115.0       5.9
     116.0       1.1
     127.0       1.9
     140.0       1.1
     155.0       1.7
     156.0       1.2
     169.0       1.2
     170.0      31.1
     171.0       4.2
     182.0       1.3
     183.0       1.0
     184.0       1.4
     198.0      84.2
     199.0      11.5
     200.0       1.1
     212.0       1.1
     213.0     100.0
     214.0      14.7
     215.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₁ N O₂	0.032 g : 0.5 ml CDCl₃
2-methoxy-3-dibenzofuranamine

    Assign.     Shift(ppm)

      A             7.755
      B             7.460
      C     *1      7.29
      D     *1      7.25
      E             7.240
      F             6.880
      G             4.0
      J             3.927

     Hz     ppm     Int.

   3103.39   7.766     94
   3102.42   7.763     87
   3101.56   7.761     74
   3096.31   7.748    111
   3094.97   7.745     96
   2986.69   7.474     93
   2985.72   7.471    102
   2979.61   7.456     93
   2978.15   7.452    119
   2922.24   7.312     47
   2920.65   7.309     51
   2914.92   7.294    113
   2913.33   7.290    102
   2907.23   7.275    111
   2905.27   7.270    164
   2903.81   7.266    112
   2897.83   7.251    135
   2896.61   7.248    134
   2893.55   7.241    334
   2890.50   7.233     66
   2889.28   7.230     55
   2887.70   7.226     53
   2749.63   6.881    353
   1569.58   3.928   1000

in CDCl3