1,1'-(1,6-hexanediyl)bisimidazole synthesis
4synthesis methods
- Product Name:1,1'-(1,6-hexanediyl)bisimidazole
- CAS Number:69506-88-3
- Molecular formula:C12H18N4
- Molecular Weight:218.3
Yield:69506-88-3 95%
Reaction Conditions:
Stage #1: 1H-imidazolewith sodium hydride in N,N-dimethyl-formamide at 0;Inert atmosphere;
Stage #2: 1 ,6-dibromohexane in N,N-dimethyl-formamide at 70; for 4 h;Inert atmosphere;
References:
Gao, Yanan;Slattery, John M.;Bruce, Duncan W. [New Journal of Chemistry,2011,vol. 35,# 12,p. 2910 - 2918] Location in patent:experimental part
