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ChemicalBook CAS DataBase List 1,1,3,3-Tetramethyldisiloxane

1,1,3,3-Tetramethyldisiloxane synthesis

9synthesis methods
-

Yield:3277-26-7 91%

Steps:

8 EXAMPLE 8

EXAMPLE 8 The procedure described in Example 7 is repeated with the modification that, instead of 0.3 g of palladium on active carbon (5% Pd), 0.02 g (1.1·10-4 mol) of palladium(II) chloride is used. The product is isolated by distillation. 46.3 g of 1,3-dichloro-1,1,3,3-tetramethyldisiloxane (91% yield, based on 1,3-dihydro-1,1,3,3-tetramethyldisiloxane) are obtained.

References:

US6284907,2001,B1

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