1-(1,3-THIAZOL-2-YL)PIPERIDINE synthesis
- Product Name:1-(1,3-THIAZOL-2-YL)PIPERIDINE
- CAS Number:4175-70-6
- Molecular formula:C8H12N2S
- Molecular Weight:168.26
110-89-4
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$15.96/100ML
3034-53-5
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$5.00/5g
4175-70-6
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$60.00/100mg
Yield:4175-70-6 100%
Reaction Conditions:
at 100; for 2.5 h;
Steps:
77
Piperidine solution (70 ml) of 1 (15.0 g 91.45 mmol) was stirred at 100°C for 2.5 hours. The reaction solution was allowed to stand to cool down and filtered to remove the insolubles, and the filtrate was evaporated to dryness under reduced pressure. The residue was purified by silica gel column chromatography (solvent: n-hexane/ethyl acetate = 9/1), to obtain 60 (15.39 g, 100%) of oily colorless substance. APCI-MS m/z 169[M+H]+
References:
EP2103611,2009,A1 Location in patent:Page/Page column 63-64
110-89-4
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$15.96/100ML
3034-52-4
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$12.00/5g
4175-70-6
24 suppliers
$60.00/100mg
110-89-4
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$15.96/100ML
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4175-70-6
24 suppliers
$60.00/100mg