1,10-Dioxacyclooctadecane-2,11-dione synthesis

5synthesis methods

Product Name:1,10-Dioxacyclooctadecane-2,11-dione
CAS Number:793-32-8
Molecular formula:C16H28O4
Molecular Weight:284.3911

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: Et₃N / CH₂Cl₂
2: 40 percent / TiCl₄, AgClO₄, p-trifluoromethylbenzoic anhydride / CH₂Cl₂ / 3 h / Ambient temperature

References:

Mukaiyama, Teruaki;Izumi, Jun;Miyashita, Mitsutomo;Shiina, Isamu [Chemistry Letters,1993,# 5,p. 907 - 910]

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5698-29-3 Synthesis

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References

17696-11-6 Synthesis

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References

1795-61-5
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References

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98-11-3
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References

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