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128520-86-5

1,2-Benzisoxazole,3-chloro-7-methyl-(9CI) synthesis

2synthesis methods
36238-83-2 Synthesis
7-METHYLBENZO[D]ISOXAZOL-3-OL

36238-83-2
47 suppliers
$29.00/50mg

1,2-Benzisoxazole,3-chloro-7-methyl-(9CI)

128520-86-5
22 suppliers
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Yield:128520-86-5 77%

Steps:

28.a 3-(2-Aminoethylthio)-7-methyl-1,2-benzisoxazole hydrochloride

(a) 3-Chloro-7-methyl-1,2-benzisoxazole. The title compound (0.30 g, 77%) was obtained from 3-hydroxy-7-methyl-1,2-benzisoxazole (0.35 g) by similar reactions and treatments as in example 26(a).

References:

US5965591,1999,A