Triethylamine synthesis
- Product Name:Triethylamine
- CAS Number:121-44-8
- Molecular formula:C6H15N
- Molecular Weight:101.19
Triethylamine is a colourless volatile liquid with a strong fishy odor reminiscent of ammonia. Triethylamine is synthesised by the alkylation of ammonia with ethanol.
87-90-1
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121-44-8
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Yield:121-44-8 80%
Reaction Conditions:
in dichloromethane
Steps:
6-n-propyl-2-formyl-8beta-ergoline-carboxylic acid methyl ester
The aldehyde is obtained from the corresponding Mannich base by oxidation with trichloroisocyanuric acid in dichloromethane and triethylamine at -78° C. in approximately 80% yield.
References:
Schering Aktiengesellschaft US5219862, 1993, A
2687-45-8
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121-44-8
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121-44-8
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121-44-8
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121-44-8
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