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ChemicalBook CAS DataBase List 1,2-BISMALEIMIDOETHANE

1,2-BISMALEIMIDOETHANE synthesis

5synthesis methods
-

Yield:5132-30-9 85%

Reaction Conditions:

in 1,1,2,2-tetrachloroethane at 120; for 12 h;

Steps:

General procedure for retro-Diels-Alder reaction

General procedure: A solution of alkylated product(1 mol) in 1,1,2,2-tetrachloroethane was stirred at 120 C in an open flask for12 h. After completion of the reaction as indicated by TLC, the solvent wasevaporated under reduced pressure to afford BMI.

References:

Rao, Venkataramanarao;Navath, Suryakiran;Kottur, Mohankumar;McElhanon, James R.;McGrath, Dominic V. [Tetrahedron Letters,2013,vol. 54,# 37,p. 5011 - 5013]

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