1-(2-CHLOROPHENYL)-1-PROPANOL 95 synthesis
- Product Name:1-(2-CHLOROPHENYL)-1-PROPANOL 95
- CAS Number:22869-35-8
- Molecular formula:C9H11ClO
- Molecular Weight:170.64
Yield:22869-35-8 93%
Reaction Conditions:
Stage #1: diethylzincwith N,N'-bis((R,R)-2-diethylaminocyclohexyl)oxalylamide in toluene at 20; for 0.5 h;Inert atmosphere;
Stage #2: 2-chloro-benzaldehyde in toluene at 20; for 24 h;Inert atmosphere;enantioselective reaction;Reagent/catalyst;
References:
Maleev;Gugkaeva;Tsaloev;Moskalenko;Khrustalev [Russian Chemical Bulletin,2012,vol. 61,# 1,p. 51 - 58][Izv. Akad. Nauk, Ser. Khim.,2012,# 1,p. 50 - 57]
6323-18-8
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$32.00/250mg
22869-35-8
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