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ChemicalBook CAS DataBase List 1 2-DIMYRISTOYL-RAC-GLYCEROL (C14:0)
20255-94-1

1 2-DIMYRISTOYL-RAC-GLYCEROL (C14:0) synthesis

10synthesis methods
-

Yield:20255-94-1 88%

Reaction Conditions:

with palladium on activated charcoal;hydrogen in ethanol at 30; for 12 h;

Steps:

1.d (d) Preparation of Compound 4

To a solution of compound 3 (20.0 g, 33.1 mmol, 1.0 eq) in EtOH (500 mL) was added Pd/C (17.6 g) and the mixture was stirred under hydrogen atmosphere at 30 °C for 12 h. The reaction was filtered and filtrated was concentrated to give compound 4 (15.0 g, 88%).

References:

WO2019/89523,2019,A1 Location in patent:Page/Page column 82

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