1-(2-METHOXYETHOXY)-2-METHYL-2-PROPANOL synthesis
- Product Name:1-(2-METHOXYETHOXY)-2-METHYL-2-PROPANOL
- CAS Number:211321-90-3
- Molecular formula:C7H16O3
- Molecular Weight:148.2
558-30-5
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$20.00/5G
109-86-4
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$11.00/25g
211321-90-3
14 suppliers
$71.70/1ml
Yield:211321-90-3 45%
Reaction Conditions:
Stage #1: 2-methoxy-ethanolwith sodium hydride in tetrahydrofuran at 0 - 20; for 0.5 h;Inert atmosphere;
Stage #2: 2-methyl-1,2-epoxypropane in tetrahydrofuran at 0 - 90; for 12 h;Inert atmosphere;
References:
George, Sheby Mary;Kim, Hyo-Suk;Oh, Hyun Ji;Lah, Myoung Soo;Jeon, Dong Ju;Park, Bo Keun;Han, Jeong Hwan;Kim, Chang Gyoun;Chung, Taek-Mo [Dalton Transactions,2015,vol. 44,# 31,p. 14042 - 14053]