1,3-BENZODIOXOLE-4-CARBOXYLIC ACID synthesis
- Product Name:1,3-BENZODIOXOLE-4-CARBOXYLIC ACID
- CAS Number:5768-39-8
- Molecular formula:C8H6O4
- Molecular Weight:166.13
7797-83-3
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$12.00/250mg
5768-39-8
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$54.00/100 mg
Yield: 96%
Reaction Conditions:
with dihydrogen peroxide;potassium carbonate in methanol;water
Steps:
22 2,3-(methylenedioxy)benzoic acid
2,3-(methylenedioxy)benzoic acid A solution of 2,3-(methylenedioxy)benzaldehyde (160mg, 1.06mmol), potassium carbonate (960 mg, 6.9 mmol) and 2.4mL of hydrogen peroxide (30-32 wt.% solution in water) in 10 mL of methanol was stirred for 16 hours at room temperature. The mixture was washed with diethyl ether. The water layer was acidified with 1 N aq. HCl to pH>1, then extracted with ethyl acetate. The organic layer was dried over MgSO4, then concentrated to give the desired product (170mg, 96%). EI-MS (m/z) 164.8 (M-).
References:
33842-16-9
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$45.00/100mg
5768-39-8
110 suppliers
$54.00/100 mg
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23158-06-7
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5768-39-8
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$5.00/5g
5768-39-8
110 suppliers
$54.00/100 mg
274-09-9
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$5.00/5g
124-38-9
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5768-39-8
110 suppliers
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