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1,3-Dibutylbenzene synthesis

4synthesis methods
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Yield:17171-74-3 86 %Spectr.

Reaction Conditions:

with [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride;lithium bromide in tetrahydrofuran;desipramine at 25; for 2 h;Inert atmosphere;chemoselective reaction;Negishi cross-coupling;

References:

Larrosa, Igor;Somoza, Clara;Banquy, Alexandre;Goldup, Stephen M. [Organic Letters,2011,vol. 13,# 1,p. 146 - 149] Location in patent:supporting information; experimental part