Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

1-(4-chlorophenyl)-3,3-dimethyltriazene synthesis

3synthesis methods
-

Yield:7203-90-9 38%

Reaction Conditions:

Stage #1: 4-chloro-anilinewith hydrogenchloride;isopentyl nitrite in water;acetonitrile at 0;Flow reactor;
Stage #2: dimethyl amine in tetrahydrofuran;water;acetonitrile at 0 - 20; for 0.333333 h;Flow reactor;

References:

Schotten, Christiane;Leprevost, Samy K.;Yong, Low Ming;Hughes, Colan E.;Harris, Kenneth D. M.;Browne, Duncan L. [Organic Process Research and Development,2020,vol. 24,# 10,p. 2336 - 2341] Location in patent:supporting information