1-(4-chlorophenyl)-3,3-dimethyltriazene synthesis
- Product Name:1-(4-chlorophenyl)-3,3-dimethyltriazene
- CAS Number:7203-90-9
- Molecular formula:C8H10ClN3
- Molecular Weight:183.64
Yield:7203-90-9 38%
Reaction Conditions:
Stage #1: 4-chloro-anilinewith hydrogenchloride;isopentyl nitrite in water;acetonitrile at 0;Flow reactor;
Stage #2: dimethyl amine in tetrahydrofuran;water;acetonitrile at 0 - 20; for 0.333333 h;Flow reactor;
References:
Schotten, Christiane;Leprevost, Samy K.;Yong, Low Ming;Hughes, Colan E.;Harris, Kenneth D. M.;Browne, Duncan L. [Organic Process Research and Development,2020,vol. 24,# 10,p. 2336 - 2341] Location in patent:supporting information
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