1-((4-CHLOROPHENYL)METHYL)-1H-PYRROLE-2,5-DIONE synthesis
- Product Name:1-((4-CHLOROPHENYL)METHYL)-1H-PYRROLE-2,5-DIONE
- CAS Number:34569-29-4
- Molecular formula:C11H8ClNO2
- Molecular Weight:221.64
108-31-6
878 suppliers
$13.47/50g
104-86-9
293 suppliers
$6.00/5g
34569-29-4
21 suppliers
$57.50/250mg
Yield:34569-29-4 82%
Reaction Conditions:
Stage #1: maleic anhydride;4-chlorobenzylamine in dichloromethane at 25; for 12 h;
Stage #2: with oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane; for 24 h;cooling;
Stage #3: with triethylamine in dichloromethane at 25; for 2 h;Further stages.;
References:
Schweizer, Eliane;Hoffmann-Roeder, Anja;Olsen, Jacob A.;Seiler, Paul;Obst-Sander, Ulrike;Wagner, Bjoern;Kansy, Manfred;Banner, David W.;Diederich, Franois [Organic and Biomolecular Chemistry,2006,vol. 4,# 12,p. 2364 - 2375]
104-88-1
647 suppliers
$5.00/25g
34569-29-4
21 suppliers
$57.50/250mg