1,4-dibromo-2,5-divinylbenzene synthesis
- Product Name:1,4-dibromo-2,5-divinylbenzene
- CAS Number:868847-75-0
- Molecular formula:C10H8Br2
- Molecular Weight:287.98
1074-24-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 44 percent / N-bromosuccinimide; 1,1'-azobis(cyclohexanecarbonitrile) / benzene / 8 h / Heating
2.1: triphenylphosphine / dimethylformamide / 18 h / Heating
2.2: 90 percent / potassium tert-butoxide / tetrahydrofuran
References:
Bonifacio, Margel C.;Robertson, Charles R.;Jung, Jun-Young;King, Benjamin T. [Journal of Organic Chemistry,2005,vol. 70,# 21,p. 8522 - 8526]
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35335-16-1
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106-42-3
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