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1-(4-FLUORO-PHENYL)-PROPANE-1,2-DIONE synthesis

5synthesis methods
-

Yield: 75%

Reaction Conditions:

with 2,2'-azobis(isobutyronitrile);oxygen;palladium diacetate;sodium carbonate at 120; under 6080.41 Torr; for 20 h;Autoclave;

References:

Wang, Azhong;Jiang, Huanfeng;Li, Xianwei [Journal of Organic Chemistry,2011,vol. 76,# 16,p. 6958 - 6961] Location in patent:supporting information; experimental part