1-4-NITROPHENOXY-2-3-PROPANEDIOL synthesis
- Product Name:1-4-NITROPHENOXY-2-3-PROPANEDIOL
- CAS Number:34211-48-8
- Molecular formula:C9H11NO5
- Molecular Weight:213.19
100-02-7
34 suppliers
$11.00/5G
556-52-5
285 suppliers
$17.67/1gm:
34211-48-8
20 suppliers
$265.00/100mg
Yield:34211-48-8 95.7%
Reaction Conditions:
with potassium hydroxide in toluene at 90; for 24 h;
Steps:
6 EXAMPLE 6
EXAMPLE 6 [00036] [C00011] [00037] The 4-Nitrophenol (300 g, 2.16 mol), toluene (240 ml) and KOH flake (0.6 g) were charged into a 1000-ml 3-neck flask and the mixture was heated to 90° C. for 30 min. After cooling down to 5° C., glycidol (192 g, 2.59 mol) was introduced through an additional funnel while stirring and the resulting mixture was heated to 90° C. for 24 hours. GC-MS found that the 4-nitrophenol was consumed. The reaction was cooling down, toluene and excess of glycidol were removed by a rotary evaporator. 440 g (95.7%) of product nitrophenoxyglycidol (structure above) was obtained.
References:
US6667392,2003,B2 Location in patent:Page column 7
100-02-7
34 suppliers
$11.00/5G
96-24-2
308 suppliers
$11.00/5g
34211-48-8
20 suppliers
$265.00/100mg
125228-75-3
1 suppliers
inquiry
34211-48-8
20 suppliers
$265.00/100mg
100-02-7
34 suppliers
$11.00/5G
556-52-5
285 suppliers
$17.67/1gm:
34211-48-8
20 suppliers
$265.00/100mg
125228-75-3
1 suppliers
inquiry
34211-48-8
20 suppliers
$265.00/100mg
125279-82-5
18 suppliers
inquiry
125279-81-4
10 suppliers
inquiry