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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
40180-70-9

1-(5-Hydroxy-2-Methylphenyl)ethanone synthesis

5synthesis methods
Preparation from 5-acetyl-4-methyl-3-cyclohexenone by aromatization promoted, ? by cupric bromide with lithium bromide in refluxing acetonitrile (80%) ; ? by 10% Pd/C in refluxing xylene (50%).
5-HYDROXY-2-METHYL-BENZOIC ACID

578-22-3
212 suppliers
$8.00/1g

Methyllithium

917-54-4
184 suppliers
$52.10/25ml

1-(5-Hydroxy-2-Methylphenyl)ethanone

40180-70-9
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Yield:40180-70-9 68%

Reaction Conditions:

in tetrahydrofuran;diethyl ether at -78 - 25; for 17 h;Inert atmosphere;

References:

Lafleur, Karine;Huang, Danzhi;Zhou, Ting;Caflisch, Amedeo;Nevado, Cristina [Journal of Medicinal Chemistry,2009,vol. 52,# 20,p. 6433 - 6446] Location in patent:experimental part

534-22-5 Synthesis
2-Methylfuran

534-22-5
313 suppliers
$10.00/5mL

1423-60-5 Synthesis
3-Butyn-2-one

1423-60-5
179 suppliers
$23.00/1g

1-(5-Hydroxy-2-Methylphenyl)ethanone

40180-70-9
18 suppliers
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References
140-39-6 Synthesis
P-TOLYL ACETATE

140-39-6
207 suppliers
$10.00/25g

106-44-5 Synthesis
p-Cresol

106-44-5
509 suppliers
$14.00/5g

1450-72-2 Synthesis
1-(2-Hydroxy-5-methylphenyl)ethanone

1450-72-2
201 suppliers
$6.00/1g

1-(5-Hydroxy-2-Methylphenyl)ethanone

40180-70-9
18 suppliers
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References
106-44-5 Synthesis
p-Cresol

106-44-5
509 suppliers
$14.00/5g

1-(5-Hydroxy-2-Methylphenyl)ethanone

40180-70-9
18 suppliers
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References
1202-08-0 Synthesis
5'-isopropyl-2'-methylacetophenone

1202-08-0
6 suppliers
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1-(5-Hydroxy-2-Methylphenyl)ethanone

40180-70-9
18 suppliers
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References