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ChemicalBook CAS DataBase List 1-BROMO-2-[(METHYLSULFANYL)METHYL]BENZENE
19614-11-0

1-BROMO-2-[(METHYLSULFANYL)METHYL]BENZENE synthesis

5synthesis methods
-

Yield:19614-11-0 86%

Reaction Conditions:

Stage #1: methylthiolwith sodium hydride in tetrahydrofuran at 0 - 20; for 1 h;
Stage #2: 1-Bromo-2-bromomethyl-benzene in tetrahydrofuran; for 16 h;Reflux;

References:

Mohy El Dine, Tharwat;Erb, William;Berhault, Yohann;Rouden, Jacques;Blanchet, Jér?me [Journal of Organic Chemistry,2015,vol. 80,# 9,p. 4532 - 4544]