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60767-73-9

1-Butanol, 4-(4-chlorobutoxy)- synthesis

4synthesis methods
-

Yield:60767-73-9 70%

Reaction Conditions:

Stage #1: 1,4-Butanediolwith sodium hydroxide in water;dimethyl sulfoxide; for 0.166667 h;
Stage #2: 4-chlorobutyl bromide in water;dimethyl sulfoxide at 20; for 18 h;

References:

Miller, Daniel S. J.;Rossanese, Olivia W.;Collins, Ian;Voell, Sabine A.;Gütschow, Michael;Steinebach, Christian;Sosi?, Izidor;Proj, Matic;Schnakenburg, Gregor [2022,vol. 13,# 6,p. 731 - 736] Location in patent:supporting information