1-Fluoro-4-(3-nitrophenyl)benzene synthesis
- Product Name:1-Fluoro-4-(3-nitrophenyl)benzene
- CAS Number:10540-32-6
- Molecular formula:C12H8FNO2
- Molecular Weight:217.2
645-00-1
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$50.00/1g
1765-93-1
551 suppliers
$9.00/1g
10540-32-6
11 suppliers
$60.00/100mg
Yield:10540-32-6 99%
Reaction Conditions:
with potassium phosphate tribasic trihydrate in toluene at 100; for 8 h;Inert atmosphere;Suzuki Coupling;
Steps:
8 Example 5: Ni(II)-α-diimine-POP catalyst catalyzes the reaction between iodobenzene and phenylboronic acid
General procedure: Iodobenzene (1.0 mmol, 116 μL), phenylboronic acid (1.1 mmol, 0.134 g), K3PO4·3H2O (2 mmol, 0.533 g), and Ni(II)-α-diimine-POP (52 mg), 2 ml of toluene was added at 100 °C. Stir for 8h under N2. The yield was determined by gas chromatography. Yield: 99%.
References:
CN110229080,2019,A Location in patent:Paragraph 0092-0093; 0106-0111
13331-27-6
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460-00-4
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$6.00/10g
10540-32-6
11 suppliers
$60.00/100mg
645-00-1
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$50.00/1g
25776-12-9
97 suppliers
$51.00/100mg
10540-32-6
11 suppliers
$60.00/100mg
645-00-1
15 suppliers
$50.00/1g
437-29-6
3 suppliers
$172.00/25MG
10540-32-6
11 suppliers
$60.00/100mg