ChemicalBook CAS DataBase List 1-N-Boc-2-Methylhydrazine

1-N-Boc-2-Methylhydrazine synthesis

3synthesis methods

Product Name:1-N-Boc-2-Methylhydrazine
CAS Number:127799-54-6
Molecular formula:C6H14N2O2
Molecular Weight:146.19

870-46-2 Synthesis

870-46-2
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127799-54-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 64 percent / toluene / 6 h
2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / cooling
2.2: tetrahydrofuran; hexane / 5 h
2.3: 83 percent / aq. NaOH / CH₂Cl₂ / 0.5 h / 20 °C

References:

Melendez, Rosa E.;Lubell, William D. [Journal of the American Chemical Society,2004,vol. 126,# 21,p. 6759 - 6764]

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127799-53-5 Synthesis

1-(benzylo×y)carbonyl-2-(t-butylo×y)carbonyl-1-Methylhydrazine

127799-53-5
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127799-54-6
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References

24424-99-5 Synthesis

24424-99-5
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$13.50/25G

127799-54-6
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References

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