1-PHENYL-1H-1,2,3-TRIAZOLE-4-CARBALDEHYDE synthesis
- Product Name:1-PHENYL-1H-1,2,3-TRIAZOLE-4-CARBALDEHYDE
- CAS Number:34296-51-0
- Molecular formula:C9H7N3O
- Molecular Weight:173.17
103755-58-4
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34296-51-0
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$90.00/50mg
Yield:34296-51-0 99%
Reaction Conditions:
with manganese(IV) oxide in dichloromethane at 20;
Steps:
27.2
Step 2 Synthesis of 1-Phenyl-1H-[1,2,3]triazole-4-carbaldehyde MnO2 (1.23 g, 14.14 mmol) was added to a stirred solution of (1-phenyl-1H-[1,2,3]triazol-4-yl)-methanol (245 mg, 1.4 mmol) in DCM (15 mL) and the resulting mixture was stirred at room temperature overnight. The mixture was filtered over a celite bed, and the filtrate was concentrated under reduced pressure to afford 271 mg (99%) of 1-phenyl-1H-[1,2,3]triazole-4-carbaldehyde.
References:
US2010/160323,2010,A1 Location in patent:Page/Page column 30
10160-87-9
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622-37-7
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34296-51-0
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34296-51-0
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113934-26-2
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62-53-3
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34296-51-0
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100-01-6
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10160-87-9
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622-37-7
42 suppliers
$45.00/100mg
34296-51-0
31 suppliers
$90.00/50mg
1012081-57-0
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