1-(PHENYLSULFONYL)-1H-INDOL-3-YLBORONIC ACID synthesis

5synthesis methods

40899-71-6 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 95 percent / Br₂ / CCl₄
2.1: t-BuLi; B(O-i-Pr)3 / tetrahydrofuran
2.2: 85 percent / Acid hydrolysis

References:

Chao, Wan-Ru;Yean, Dawn;Amin, Khalid;Green, Carol;Jong, Ling [Journal of Medicinal Chemistry,2007,vol. 50,# 15,p. 3412 - 3415]

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