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ChemicalBook CAS DataBase List Pazinaclone
103255-66-9

Pazinaclone synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: benzotriazol-1-ol; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Schlenk technique; Inert atmosphere
2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate; potassium carbonate / 1,4-dioxane / 80 °C / Schlenk technique; Inert atmosphere

References:

Liu, Cong;Zhang, Qi;Li, Hongbo;Guo, Shuangxi;Xiao, Bin;Deng, Wei;Liu, Lei;He, Wei [Chemistry - A European Journal,2016,vol. 22,# 18,p. 6208 - 6212]

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