N-Boc-L-homoserine Methyl Ester 4-Methylbenzenesulfonate synthesis
- Product Name:N-Boc-L-homoserine Methyl Ester 4-Methylbenzenesulfonate
- CAS Number:120042-09-3
- Molecular formula:C17H25NO7S
- Molecular Weight:387.45
98-59-9
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$9.00/5g
120042-11-7
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$75.00/100mg
120042-09-3
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$65.00/10mg
Yield:120042-09-3 7.8 g
Reaction Conditions:
with dmap;triethylamine in dichloromethane at 0 - 20; for 2 h;
Steps:
7.1 step 1:
Dissolve SMA24 (4.66g), TEA (2.42g), DMAP (0.24g) in DCM (50mL),The temperature was lowered to 0° C., TsCl (4 g) was added in batches, and then reacted at room temperature for 2 hours. Water (30 mL) was added, the liquids were separated, and the organic phase was spin-dried to obtain 7.8 g of the product.
References:
CN112552348,2021,A Location in patent:Paragraph 0379-0384
24424-99-5
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120042-09-3
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$65.00/10mg
41088-86-2
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$24.00/1g
120042-09-3
16 suppliers
$65.00/10mg