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ChemicalBook CAS DataBase List (4S)-4-t-Butyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester
1206227-45-3

(4S)-4-t-Butyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: sodium carbonate / tetrahydrofuran; water / Cooling with ice
2: thionyl chloride; pyridine / acetonitrile / 3 h / -40 - 20 °C / Inert atmosphere
3: rhodium(III) chloride hydrate; sodium periodate / water; acetonitrile / 1 h / 0 - 20 °C

References:

Dong, Ze;Yan, Chao;Gao, Yongzhi;Dong, Chune;Qiu, Guofu;Zhou, Hai-Bing [Advanced Synthesis and Catalysis,2015,vol. 357,# 9,p. 2132 - 2142]

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