2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene synthesis
- Product Name:2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene
- CAS Number:1289556-30-4
- Molecular formula:C21H30S3Sn3
- Molecular Weight:734.79
Yield:1289556-30-4 100%
Reaction Conditions:
Stage #1: benzo(1,2-b;3,4-b′;5,6-b′′)trithiophene in tetrahydrofuran;hexane at 0 - 20; for 6 h;Inert atmosphere;
Stage #2: trimethyltin(IV)chloride in tetrahydrofuran;hexane at 20;Inert atmosphere;
References:
Kashiki, Tomoya;Kohara, Masahiro;Osaka, Itaru;Miyazaki, Eigo;Takimiya, Kazuo [Journal of Organic Chemistry,2011,vol. 76,# 10,p. 4061 - 4070] Location in patent:experimental part
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351014-15-8
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151721-79-8
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