ChemicalBook CAS DataBase List 2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene

2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene synthesis

6synthesis methods

Product Name:2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene
CAS Number:1289556-30-4
Molecular formula:C21H30S3Sn3
Molecular Weight:734.79

29150-63-8 Synthesis

29150-63-8
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1066-45-1
147 suppliers
$31.50/2g

2,5,8-Tris(trimethylstannyl)benzo[1,2-b:3,4-b':5,6-b'']trithiophene

1289556-30-4
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Yield:1289556-30-4 100%

Reaction Conditions:

Stage #1: benzo(1,2-b;3,4-b′;5,6-b′′)trithiophene in tetrahydrofuran;hexane at 0 - 20; for 6 h;Inert atmosphere;
Stage #2: trimethyltin(IV)chloride in tetrahydrofuran;hexane at 20;Inert atmosphere;

References:

Kashiki, Tomoya;Kohara, Masahiro;Osaka, Itaru;Miyazaki, Eigo;Takimiya, Kazuo [Journal of Organic Chemistry,2011,vol. 76,# 10,p. 4061 - 4070] Location in patent:experimental part

1,3,5-trichloro-2,4,6-tris[(trimethylsilyl)ethynyl]benzene

351014-15-8
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1289556-30-4
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References

151721-79-8
43 suppliers
$68.00/200mg

1289556-30-4
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References

108-70-3 Synthesis

108-70-3
245 suppliers
$21.00/100g

1289556-30-4
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References

108-73-6
488 suppliers
$13.00/5g

1289556-30-4
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References