17 alpha-cyanomethyl-19-nortestosterone synthesis
- Product Name:17 alpha-cyanomethyl-19-nortestosterone
- CAS Number:67473-36-3
- Molecular formula:C20H27NO2
- Molecular Weight:313.43
17976-34-0
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67473-36-3
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Yield:67473-36-3 74%
Steps:
11 13-Methyl-17α-cyanomethyl-17β-hydroxy-4-gonen-3-one
EXAMPLE 11 13-Methyl-17α-cyanomethyl-17β-hydroxy-4-gonen-3-one 3.0 g 3-methoxy-13-methyl-3,5-gonadiene-17-one are converted in a manner analogous to that in Example 6. Yield: 74% of theory Flame point: 243° to 246° C. 1 H-NMR spectrum: (80 MHz, CDCl3, δ against TMS as inner standard) 0.84 ppm (s, 3H, 18--CH3); 2.63 ppm (2d, 2H 17α--CH2 CN); 5.75 ppm (s, 1H, 4--CH).
References:
US5438134,1995,A
65928-64-5
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67473-36-3
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![Spiro[estra-2,5(10)-diene-17,2'-oxirane], 4-methoxy-, (17β)- (9CI)](/CAS/20210305/GIF/30925-89-4.gif)
30925-89-4
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67473-36-3
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