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17615-10-0

2-Butenoic acid, 4-(4-methoxyphenyl)-4-oxo-, methyl ester synthesis

3synthesis methods
-

Yield:17615-10-0 82%

Reaction Conditions:

with toluene-4-sulfonic acid;1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide at 65; for 50 h;

References:

Li, Ziyuan;Wang, Yiyun;Tang, Changhua;Xu, Jinyi;Wu, Xiaoming;Yao, Hequan [Chinese Journal of Chemistry,2010,vol. 28,# 7,p. 1301 - 1305] Location in patent:experimental part