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Ethanone, 2,2-difluoro-2-(methylthio)-1-phenyl- (9CI) synthesis

4synthesis methods
-

Yield:192862-16-1 82%

Reaction Conditions:

with 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate;zinc dibromide in 1,1,2-trichloroethane at 80 - 105;

References:

Eto;Kaneko;Takeda;Tokizawa;Sato;Yoshida;Namiki;Ogawa;Maebashi;Ishida;Matsumoto;Asaoka [Chemical and Pharmaceutical Bulletin,2001,vol. 49,# 2,p. 173 - 182]