ChemicalBook CAS DataBase List 1H-Indole-2-carbonitrile,3-methyl-

1H-Indole-2-carbonitrile,3-methyl- synthesis

11synthesis methods

Product Name:1H-Indole-2-carbonitrile,3-methyl-
CAS Number:13006-59-2
Molecular formula:C10H8N2
Molecular Weight:156.18

83-34-1 Synthesis

83-34-1
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13006-59-2
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: LDA / tetrahydrofuran / -78 °C
1.2: 85 percent / tetrahydrofuran
2.1: LDA / tetrahydrofuran / -78 °C
2.2: 68 percent / tetrahydrofuran
3.1: 83 percent / POCl₃ / benzene
4.1: 72 percent / NaH; PhSH / tetrahydrofuran / Heating

References:

Denison, Sophie;Hilton, Stephen T. [Synlett,2004,# 15,p. 2806 - 2808]

1H-Indole-2-carboxamide, N-(1,1-dimethylethyl)-3-methyl-

17537-57-4
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13006-59-2
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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13006-59-2
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References

1H-Indole-2-carbonitrile, 3-methyl-1-(phenylsulfonyl)-

838874-62-7
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13006-59-2
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References

1000210-73-0
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13006-59-2
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References

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