1H-Pyrrolo[3,2-b]pyridine-5-methanamine(9CI) synthesis
- Product Name:1H-Pyrrolo[3,2-b]pyridine-5-methanamine(9CI)
- CAS Number:267876-26-6
- Molecular formula:C8H9N3
- Molecular Weight:147.18
Yield:-
Reaction Conditions:
Stage #1: 6-methyl-5-nitropyridine-2-carbonitrile;N,N-dimethyl-formamide dimethyl acetal in N,N-dimethyl-formamide at 90; for 2 h;
Stage #2: with hydrogenchloride;methanol;palladium on activated charcoal for 16 h;
References:
Sanderson, Philip E. J.;Stanton, Matthew G.;Dorsey, Bruce D.;Lyle, Terry A.;McDonough, Colleen;Sanders, William M.;Savage, Kelly L.;Naylor-Olsen, Adel M.;Krueger, Julie A.;Lewis, S. Dale;Lucas, Bobby J.;Lynch, Joseph J.;Yan, Youwei [Bioorganic and Medicinal Chemistry Letters,2003,vol. 13,# 5,p. 795 - 798]
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