2-(2-Bromo-5-chlorophenyl)acetaldehyde synthesis
- Product Name:2-(2-Bromo-5-chlorophenyl)acetaldehyde
- CAS Number:265107-67-3
- Molecular formula:C8H6BrClO
- Molecular Weight:233.49
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 1,1,1,3,3,3-hexamethyldisilazane potassium / toluene / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 7 h / 0 - 20 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; lithium hydroxide monohydrate / 12 h / Reflux
References:
Wurst, Jacqueline M.;Liu, Guodong;Tan, Derek S. [Journal of the American Chemical Society,2011,vol. 133,# 20,p. 7916 - 7925]
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