2-(2-methoxyethoxy)acetaldehyde synthesis
- Product Name:2-(2-methoxyethoxy)acetaldehyde
- CAS Number:111964-99-9
- Molecular formula:C5H10O3
- Molecular Weight:118.13
111-77-3
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Yield:111964-99-9 2.83 mg
Reaction Conditions:
Stage #1: 2-(2-methoxyethoxy)ethyl alcoholwith oxalyl dichloride;dimethyl sulfoxide in tetrahydrofuran at -78; for 0.5 h;Inert atmosphere;Swern Oxidation;
Stage #2: with triethylamine in tetrahydrofuran at -78 - 20; for 0.25 h;Inert atmosphere;Swern Oxidation;
References:
Seifert, Tina;Malo, Marcus;Kokkola, Tarja;Engen, Karin;Fridén-Saxin, Maria;Wallén, Erik A. A.;Lahtela-Kakkonen, Maija;Jarho, Elina M.;Luthman, Kristina [Journal of Medicinal Chemistry,2014,vol. 57,# 23,p. 9870 - 9888]
62005-54-3
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111964-99-9
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109-86-4
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