ChemicalBook CAS DataBase List 2-(3-chlorobenzoyl)benzoic acid

2-(3-chlorobenzoyl)benzoic acid synthesis

5synthesis methods

Product Name:2-(3-chlorobenzoyl)benzoic acid
CAS Number:13450-37-8
Molecular formula:C14H9ClO3
Molecular Weight:260.67

6268-18-4
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13450-37-8
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Yield:13450-37-8 77%

Reaction Conditions:

Stage #1: 2-(3-amino-benzoyl)-benzoic acidwith sulfuric acid;sodium nitrite in water at 0; for 1 h;
Stage #2: with hydrogenchloride;copper(l) chloride in water at 20;

References:

Bond, Silas;Draffan, Alistair G.;Fenner, Jennifer E.;Lambert, John;Lim, Chin Yu;Lin, Bo;Luttick, Angela;Mitchell, Jeffrey P.;Morton, Craig J.;Nearn, Roland H.;Sanford, Vanessa;Stanislawski, Pauline C.;Tucker, Simon P. [Bioorganic and Medicinal Chemistry Letters,2015,vol. 25,# 4,p. 969 - 975]

85-44-9 Synthesis