2-(3-chlorobenzoyl)benzoic acid synthesis
- Product Name:2-(3-chlorobenzoyl)benzoic acid
- CAS Number:13450-37-8
- Molecular formula:C14H9ClO3
- Molecular Weight:260.67
6268-18-4
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13450-37-8
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Yield:13450-37-8 77%
Reaction Conditions:
Stage #1: 2-(3-amino-benzoyl)-benzoic acidwith sulfuric acid;sodium nitrite in water at 0; for 1 h;
Stage #2: with hydrogenchloride;copper(l) chloride in water at 20;
References:
Bond, Silas;Draffan, Alistair G.;Fenner, Jennifer E.;Lambert, John;Lim, Chin Yu;Lin, Bo;Luttick, Angela;Mitchell, Jeffrey P.;Morton, Craig J.;Nearn, Roland H.;Sanford, Vanessa;Stanislawski, Pauline C.;Tucker, Simon P. [Bioorganic and Medicinal Chemistry Letters,2015,vol. 25,# 4,p. 969 - 975]
26767-07-7
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65-85-0
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13450-37-8
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$370.00/1g
85-52-9
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13450-37-8
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2159-38-8
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13450-37-8
20 suppliers
$370.00/1g