2,4,6-TRINITROPHENYLHYDRAZINE synthesis
- Product Name:2,4,6-TRINITROPHENYLHYDRAZINE
- CAS Number:653-49-6
- Molecular formula:C6H5N5O6
- Molecular Weight:243.13
88-88-0
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653-49-6
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Yield:653-49-6 88%
Reaction Conditions:
with hydrazine hydrate in methanol; for 0.5 h;Reflux;
Steps:
Preparation of energetic materials
General procedure: 2.47 g (0.01 mol) picryl chloride was dissolved in 50 mL MeOH. The solution was heated until boiling, and the solution of 0.005 mol of the corresponding diamine in10 mL MeOH was added to the mixture drop by drop [11, 13]. These diamines are hydrazine, 1,2-diaminoethane,1,3-diaminopropane, 1,4-diaminobutane and 1,7-diamino-heptane, respectively. The mixture was refluxed for about 2 h, and the precipitate was filtered [4, 8]. The product was recrystallized in MeCN. Following are the characterization results of the products:
References:
Atakol, Melike;Atakol, Arda;Yigiter, Aynur ?zler;Svoboda, Ingrid;Atakol, Orhan [Journal of Thermal Analysis and Calorimetry,2017,vol. 127,# 3,p. 1931 - 1940]
606-35-9
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88-88-0
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64-17-5
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$10.00/50g
7803-57-8
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$22.78/50g
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