2-(4-Hydroxyphenyl)benzo[b]thiophene-6-ol synthesis
- Product Name:2-(4-Hydroxyphenyl)benzo[b]thiophene-6-ol
- CAS Number:63676-22-2
- Molecular formula:C14H10O2S
- Molecular Weight:242.29
63675-74-1
283 suppliers
$5.00/250mg
63676-22-2
137 suppliers
$40.00/1mg
Yield: 89.3%
Reaction Conditions:
with boron tribromide in dichloromethane at 0 - 5;
Steps:
1.1 Step one
Necked flask was charged with 0.056 mol (1-a) of 15.12 g,Dichloromethane 200 g,The reaction solution was cooled to 0-5 ° C,Boron tribromide 0.067 mol 16.87 g,The reaction was over night.The reaction solution was poured into a beaker containing 500 g of water,Dispensing.The aqueous phase was extracted three times with 300 g of dichloromethane.The organic phase was washed twice with 300 g of water.The organic phase was evaporated to dryness,Yielding 12.1 g of product 1-b,Yield: 89.3%Directly into the next step.
References:
Shijiazhuang Chengzhi Yonghua Display Materials Co., Ltd.;Yuan, Guoliang;Deng, Jia;Zhang, Fangmiao;Meng, Jinsong CN105753837, 2016, A Location in patent:Paragraph 0084; 0085; 0086; 0087; 0088
15570-12-4
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$17.00/1g
63676-22-2
137 suppliers
$40.00/1mg
2632-13-5
370 suppliers
$5.00/25mg
63676-22-2
137 suppliers
$40.00/1mg
90560-10-4
95 suppliers
$45.00/50mg
63676-22-2
137 suppliers
$40.00/1mg
![6-METHOXYBENZO[B]THIOPHENE-2-BORONIC ACID](/CAS/GIF/182133-35-3.gif)
182133-35-3
27 suppliers
$105.00/50mg
63676-22-2
137 suppliers
$40.00/1mg