Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2,5-DICHLORO-2,5-DIMETHYLHEXANE
6223-78-5

2,5-DICHLORO-2,5-DIMETHYLHEXANE synthesis

11synthesis methods
2,5-Dimethyl-2,5-hexanediol

110-03-2

2,5-DICHLORO-2,5-DIMETHYLHEXANE

6223-78-5

2,5-Dimethyl-2,5-hexanediol was used as a raw material to synthesize 2,5-dichloro-2,5-dimethylhexane (Compound 2) by the method reported by Bruson H et al (J Am Chem Soc, 62:36, 1940). The procedure was as follows: 50 g of 2,5-dimethylhexane-2,5-diol (compound 1) was reacted with 1 L of concentrated hydrochloric acid. Upon completion of the reaction, the product was quantitatively measured to determine the yield. The physical and chemical properties of the resulting compound 2 were consistent with the data reported in the literature by Bruson et al.

-

Yield:6223-78-5 100%

Reaction Conditions:

with hydrogenchloride in water

Steps:


2,5-Dichloro-2,5-dimethylhexane (compound 2) was synthesized using a known procedure set forth in Bruson H et al., J Am Chem Soc, 62:36 (1940), whereby 50 g of 2,5-dimethylhexane-2,5-diol (compound 1 ) and 1 L of concentrated hydrochloric acid was used. Yield was measured quantitatively. Properties of compound 2 matched that reported in Bruson et al.

References:

WISCONSIN ALUMNI RESEARCH FOUNDATION WO2007/5568, 2007, A1 Location in patent:Page/Page column 10

FullText

2,5-DICHLORO-2,5-DIMETHYLHEXANE Related Search: