2-BROMO-3,5-DINITROPYRIDINE synthesis
- Product Name:2-BROMO-3,5-DINITROPYRIDINE
- CAS Number:16420-30-7
- Molecular formula:C5H2BrN3O4
- Molecular Weight:247.99
223463-14-7
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Yield:-
Reaction Conditions:
Stage #1: 6-bromopyridin-3-ylboronic acidwith potassium hydrogen bifluoride in methanol;water at 0 - 20; for 0.0333333 h;Inert atmosphere;
Stage #2: with nitrosonium tetrafluoroborate in acetonitrile at 20; for 0.00833333 h;
References:
Molander, Gary A.;Cavalcanti, Livia N. [Journal of Organic Chemistry,2012,vol. 77,# 9,p. 4402 - 4413] Location in patent:experimental part
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