2-METHYL DECANAL synthesis
- Product Name:2-METHYL DECANAL
- CAS Number:19009-56-4
- Molecular formula:C11H22O
- Molecular Weight:170.29
111-66-0
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124-19-6
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19009-56-4
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Yield:-
Reaction Conditions:
with [Rh(CO){P(CH2CH2PPh2)3}]Cl;hydrogen in dichloromethane at 80; under 26252.6 Torr; for 5 h;Catalytic behavior;Overall yield = 71 %; regioselective reaction;Reagent/catalyst;
Steps:
Catalytic activity towards hydroformylation reaction
Catalytic activity towards hydroformylation reactionThe hydroformylation reactions were carried out in a Parr reac-tor. 2.5 mmol of the alkene and 0.005 mmol of the catalyst in 5 cm3DCM were placed in a 50 cm3reaction vessel. The reaction mixturewas purged with CO/H2(1:1) for about 5 min. The CO/H2pressurewas increased to 35 bar (actual pressure) at 25C in the closed reac-tor. The hydroformylation reactions were carried out at 80 ± 2C for3-8 h at 35 ± 2 bar. The reaction mixture was analyzed by GC andproducts were isolated by column chromatography taking hexaneand ethyl acetate as eluents.
References:
Saikia, Kokil;Deb, Biswajit;Dutta, Dipak Kumar [Journal of Molecular Catalysis A: Chemical,2014,vol. 381,p. 188 - 193]
872-05-9
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19009-56-4
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112-44-7
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18675-24-6
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19009-56-4
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872-05-9
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201230-82-2
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124-18-5
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19009-56-4
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112-44-7
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$15.00/25g
29619-64-5
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19009-56-4
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