2-(Methylamino)benzophenone synthesis
- Product Name:2-(Methylamino)benzophenone
- CAS Number:1859-76-3
- Molecular formula:
- Molecular Weight:0
100-61-8
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Yield:1859-76-3 87%
Reaction Conditions:
with boron trichloride in benzonitrile;benzene;
Steps:
24 EXAMPLE 24
EXAMPLE 24 To a solution of N-methylaniline (277 mg) in benzene (5 ml), a solution of boron trichloride (303 mg) in benzene (2 ml) is added, and the resultant mixture is refluxed for 4 hours under nitrogen atmosphere. The reaction mixture is evaporated to remove the solvent. To the residue is added benzonitrile (1 ml), and the mixture is heated on a water bath at 100° C. for 4 hours. The reaction mixture is treated as in Example 5 to give 2-methylaminobenzophenone (477 mg) as crystals melting at 66° to 68° C. The yield is 87%.
References:
US4160784,1979,A
![2-[methyl(phenylsulfonyl)amino]benzoic acid](/CAS/GIF/34837-68-8.gif)
34837-68-8
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