2-Methyloxazole-4-carbonitrile synthesis
- Product Name:2-Methyloxazole-4-carbonitrile
- CAS Number:89282-09-7
- Molecular formula:C5H4N2O
- Molecular Weight:108.1
Yield:89282-09-7 10.9 g
Reaction Conditions:
Stage #1: N-cyanomethyl-acetimidic acid ethyl ester;formic acid ethyl esterwith potassium tert-butylate in dichloromethane at 0; for 1.5 h;
Stage #2: with chloro-trimethyl-silane in dichloromethane; for 1.5 h;Reflux;
References:
Benoit, Georges-Emmanuel;Carey, John S.;Chapman, Alan M.;Chima, Ranjit;Hussain, Nigel;Popkin, Matthew E.;Roux, Guillaume;Tavassoli, Bahareh;Vaxelaire, Carine;Webb, Michael R.;Whatrup, David [Organic Process Research and Development,2008,vol. 12,# 1,p. 88 - 95]
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