2-NITROSO-5-DIETHYLAMINOPHENOL HYDROCHLORIDE synthesis
- Product Name:2-NITROSO-5-DIETHYLAMINOPHENOL HYDROCHLORIDE
- CAS Number:25953-06-4
- Molecular formula:C10H15ClN2O2
- Molecular Weight:230.69
91-68-9
279 suppliers
$9.00/25g
110-46-3
291 suppliers
$10.00/10g
25953-06-4
36 suppliers
$145.00/500mg
Yield: 71%
Reaction Conditions:
in propan-1-ol
Steps:
1 5-Diethylamino-2-nitrosophenol hydrochloride
EXAMPLE 1 5-Diethylamino-2-nitrosophenol hydrochloride 0.1 mol of 3-diethylaminophenol are dissolved in 50 ml of n-propanol saturated with gaseous hydrogen chloride and, at 0° C., admixed dropwise and with stirring with 0.1 mol of isoamyl nitrite. Stirring is continued for another hour and the reaction solution is then admixed with diethyl ether, and the product which is formed is isolated by filtration with suction. Yield: 71%, m.p.: 175-177° C.
References:
Siemens Aktiengesellschaft US6284889, 2001, B1
91-68-9
279 suppliers
$9.00/25g
25953-06-4
36 suppliers
$145.00/500mg
591-27-5
531 suppliers
$11.00/10g
25953-06-4
36 suppliers
$145.00/500mg