2-Phenoxyethyl Acrylate synthesis
- Product Name:2-Phenoxyethyl Acrylate
- CAS Number:48145-04-6
- Molecular formula:C11H12O3
- Molecular Weight:192.21
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Yield:-
Reaction Conditions:
copper(I) chloride in benzene
Steps:
2 (Compound No. 23)
EXAMPLE 2 β-phenoxyethylacrylate (Compound No. 23) This compound was prepared according to a known process (Chemical Abstracts Vol. 59, 11323a). Namely, acrylic acid-chloride (5g) was added slowly under ice cooling into the mixture of β-phenoxyethylalcohol (6.75g), sodium-carbonate (2.9g), cuprous chloride (0.2g) and benzene (50ml) with stirring. The mixture was allowed to stand 15 hours at room temperature and then refluxed for 4 hours. The reaction mixture was treated according to the above mentioned known process, giving a crude product (6.6g). The crude product on fractionation gave a fraction (4.7g), b.p. 88.0° C./0.1mmHg, of β-phenoxy-ethyl acrylate.
References:
Nissan Chemical Industries, Ltd. US4036984, 1977, A
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48145-04-6
267 suppliers
$6.00/25g
122-99-6
783 suppliers
$8.00/100g
814-68-6
401 suppliers
$21.21/5gm:
48145-04-6
267 suppliers
$6.00/25g
122-99-6
783 suppliers
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48145-04-6
267 suppliers
$6.00/25g