2-tert-Butylphenazine synthesis
- Product Name:2-tert-Butylphenazine
- CAS Number:6479-87-4
- Molecular formula:C16H16N2
- Molecular Weight:236.31
62-53-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: oxone||potassium monopersulfate triple salt / dichloromethane; water / 20 °C / Inert atmosphere
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; zinc trifluoromethanesulfonate; acetic acid / 1,2-dichloro-ethane / 24 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube
References:
Xiao, Yan;Wu, Xiaopeng;Wang, Hepan;Sun, Song;Yu, Jin-Tao;Cheng, Jiang [Organic Letters,2019,vol. 21,# 8,p. 2565 - 2568]
![Diazene, 1,2-bis[4-(1,1-dimethylethyl)phenyl]-](/CAS/20210305/GIF/7775-81-7.gif)
769-92-6
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1943-67-5
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