3-BENZYLOXYISOXAZOLE-5-CARBOXYLIC ACID METHYL ESTER synthesis
- Product Name:3-BENZYLOXYISOXAZOLE-5-CARBOXYLIC ACID METHYL ESTER
- CAS Number:205115-22-6
- Molecular formula:C12H11NO4
- Molecular Weight:233.22
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 2,2'-azobis(isobutyronitrile); bromine / dichloromethane / 1 h / 35 - 40 °C / Large scale
2.1: 2,2'-azobis(isobutyronitrile); bromine / dichloromethane; water / 5 h / 35 - 40 °C / Large scale
2.2: 7 h / 35 - 45 °C / Inert atmosphere; Large scale
3.1: N-hydroxyurea; potassium tert-butylate / methanol / 17 h / -20 - 30 °C / Large scale
4.1: base / acetone
References:
Zhang, Wu-Yan;Hogan, Philip C.;Chen, Chi-Li;Niu, John;Wang, Zhimin;Lafrance, Danny;Gilicky, Olga;Dunwoody, Nicholas;Ronn, Magnus [Organic Process Research and Development,2015,vol. 19,# 11,p. 1784 - 1795]
100-39-0
438 suppliers
$10.00/10 g
10068-07-2
188 suppliers
$12.00/250mg
205115-22-6
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100-44-7
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$13.50/250G
10068-07-2
188 suppliers
$12.00/250mg
205115-22-6
21 suppliers
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100-39-0
438 suppliers
$10.00/10 g
10068-07-2
188 suppliers
$12.00/250mg
205115-22-6
21 suppliers
inquiry
205115-33-9
5 suppliers
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624-48-6
386 suppliers
$7.00/25g
205115-22-6
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